{"id":1183,"date":"2024-04-11T14:38:39","date_gmt":"2024-04-11T11:38:39","guid":{"rendered":"https:\/\/sisu.ut.ee\/lcms_method_validation\/bonus-self-test-9-5\/"},"modified":"2024-04-11T14:38:39","modified_gmt":"2024-04-11T11:38:39","slug":"bonus-self-test-9-5","status":"publish","type":"page","link":"https:\/\/sisu.ut.ee\/lcms_method_validation\/bonus-self-test-9-5\/","title":{"rendered":"Bonus self test 9.5"},"content":{"rendered":"<div id=\"watupro_quiz\" class=\"quiz-area single-page-quiz\">\n<p id=\"submittingExam33\" style=\"display:none;text-align:center;\"><img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\"><\/p>\n\n\n\n<form action=\"\" method=\"post\" class=\"quiz-form\" id=\"quiz-33\" enctype=\"multipart\/form-data\">\n<div class=\"watu-question \" id=\"question-1\" style=\";\"><div id=\"questionWrap-1\" class=\"   watupro-question-id-132\">\n\t\t\t<div class=\"question-content\"><p><span class=\"watupro_num\">1. <\/span>Estimate CC<sub>\u03b1<\/sub> and CC<sub>\u03b2<\/sub> for LC-MS\/MS measurements of triazophos from tomatoes using the method given in ISO 11843-2. Use ValChrom to estimate CC<sub>\u03b1<\/sub> and CC<sub>\u03b2<\/sub>. For those who want to understand the calculation processes behind CC<sub>\u03b1<\/sub> and CC<sub>\u03b2, <\/sub>full calculation logic can be found at [ref 18].<\/p>\n<table style=\"border-collapse: collapse;\" border=\"1\">\n<tbody>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><strong><em>c<\/em><sub>triasophos<\/sub> (mg\/kg)<\/strong><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><strong><span lang=\"EN-US\">Parallel 1<\/span><\/strong><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><strong><span lang=\"EN-US\">Parallel 2<\/span><\/strong><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><strong><span lang=\"EN-US\">Parallel 3<\/span><\/strong><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><strong><span lang=\"EN-US\">Parallel 4<\/span><\/strong><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">0<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">495<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">2834<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">1687<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">306<\/span><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">8.04E-06<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">419<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">981<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">1777<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">2141<\/span><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">9.78E-05<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">3177<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">6228<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">2803<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">4933<\/span><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">5.21E-04<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">11740<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">15274<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">13275<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">16857<\/span><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">1.21E-03<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">31638<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">37982<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">25181<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">32632<\/span><\/td>\n<\/tr>\n<tr>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"144\"><span lang=\"EN-US\">2.83E-03<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">60897<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">60702<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">60501<\/span><\/td>\n<td style=\"border: 1px solid black; padding: 5px; text-align: center;\" nowrap width=\"77\"><span lang=\"EN-US\">63998<\/span><\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p>\u00a0<\/p>\n<p>For use with ValChrom: <a href=\"https:\/\/sisu.ut.ee\/lcms_method_validation\/cca_and_ccb_4_parallels.csv\" data-fid=\"57425\">cca_and_ccb_4_parallels.csv<\/a><\/p>\n<p>Use \u03b1=\u03b2=5% and K=4 during upload.<\/p>\n<p style=\"text-align: left;\">Write results with 3 significant digits.<\/p>\n<p style=\"text-align: left;\">Estimation for CC<sub>\u03b1<\/sub>: <input type=\"text\" size=\"10\" name=\"gap_132_1\" class=\"watupro-gap answer answerof-132\" value=\"\"> (Enter your answer here)<\/p>\n<p style=\"text-align: left;\">Estimation for CC<sub>\u03b2<\/sub>: <input type=\"text\" size=\"10\" name=\"gap_132_2\" class=\"watupro-gap answer answerof-132\" value=\"\"> (Enter your answer here)<\/p>\n<input type=\"hidden\" name=\"question_id[]\" id=\"qID_1\" value=\"132\" class=\"watupro-question-id\"><input type=\"hidden\" id=\"answerType132\" class=\"answerTypeCnt1\" value=\"gaps\"><!-- end question-content--><\/div><!-- end questionWrap--><\/div>\t\t\t\t\t<div style=\"display:none;\" id=\"liveResult-1\">\t\t   \n\t\t\t\t\t\t<img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\" alt=\"Loading...\" title=\"Loading...\">\u00a0Loading...\t\t\t\t\t<\/div>\t\n\t\t\t<\/div> \n\t   \t<p id=\"liveResBtn-132\" style=\"clear:both;\"><input type=\"button\" id=\"liveResultBtn132\" class=\"liveResultBtn1 watupro-live-result-btn\" value=\"See Answer\" onclick=\"WatuPRO.liveResult(132, 1);\"><\/p>\n\t   <div class=\"watu-question \" id=\"question-2\" style=\";\"><div id=\"questionWrap-2\" class=\"   watupro-question-id-133\">\n\t\t\t<div class=\"question-content\"><p><span class=\"watupro_num\">2. <\/span>Estimate LoD from the same given data using ICH method based on calibration graph and residual deviation of residuals.<\/p>\n<p>Write results with 3 significant digits.<\/p>\n<p><input type=\"text\" size=\"10\" name=\"gap_133_1\" class=\"watupro-gap answer answerof-133\" value=\"\"> (Enter your answer here)<\/p>\n<input type=\"hidden\" name=\"question_id[]\" id=\"qID_2\" value=\"133\" class=\"watupro-question-id\"><input type=\"hidden\" id=\"answerType133\" class=\"answerTypeCnt2\" value=\"gaps\"><!-- end question-content--><\/div><!-- end questionWrap--><\/div>\t\t\t\t\t<div style=\"display:none;\" id=\"liveResult-2\">\t\t   \n\t\t\t\t\t\t<img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\" alt=\"Loading...\" title=\"Loading...\">\u00a0Loading...\t\t\t\t\t<\/div>\t\n\t\t\t<\/div> \n\t   \t<p id=\"liveResBtn-133\" style=\"clear:both;\"><input type=\"button\" id=\"liveResultBtn133\" class=\"liveResultBtn2 watupro-live-result-btn\" value=\"See Answer\" onclick=\"WatuPRO.liveResult(133, 2);\"><\/p>\n\t   <div class=\"watu-question \" id=\"question-3\" style=\";\"><div id=\"questionWrap-3\" class=\"   watupro-question-id-134\">\n\t\t\t<div class=\"question-content\"><div><span class=\"watupro_num\">3. <\/span>Which guideline is more conservative at its estimate of detection capabilities: ICH or ISO?<\/div><input type=\"hidden\" name=\"question_id[]\" id=\"qID_3\" value=\"134\" class=\"watupro-question-id\"><input type=\"hidden\" id=\"answerType134\" class=\"answerTypeCnt3\" value=\"radio\"><!-- end question-content--><\/div><div class=\"question-choices watupro-choices-columns \" id=\"questionChoices134\"><div class=\"watupro-question-choice  \" dir=\"auto\"><input type=\"radio\" name=\"answer-134[]\" id=\"answer-id-342\" class=\"answer   answerof-134 \" value=\"342\"><label for=\"answer-id-342\" id=\"answer-label-342\" class=\" answer\"><span><p>ICH<\/p><\/span><\/label><\/div><div class=\"watupro-question-choice  \" dir=\"auto\"><input type=\"radio\" name=\"answer-134[]\" id=\"answer-id-343\" class=\"answer   answerof-134 \" value=\"343\"><label for=\"answer-id-343\" id=\"answer-label-343\" class=\" answer\"><span><p>ISO<\/p><\/span><\/label><\/div><!-- end question-choices--><\/div><!-- end questionWrap--><\/div>\t\t\t\t\t<div style=\"display:none;\" id=\"liveResult-3\">\t\t   \n\t\t\t\t\t\t<img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\" alt=\"Loading...\" title=\"Loading...\">\u00a0Loading...\t\t\t\t\t<\/div>\t\n\t\t\t<\/div> \n\t   \t<p id=\"liveResBtn-134\" style=\"clear:both;\"><input type=\"button\" id=\"liveResultBtn134\" class=\"liveResultBtn3 watupro-live-result-btn\" value=\"See Answer\" onclick=\"WatuPRO.liveResult(134, 3);\"><\/p>\n\t   <div class=\"watu-question \" id=\"question-4\" style=\";\"><div id=\"questionWrap-4\" class=\"   watupro-question-id-135\">\n\t\t\t<div class=\"question-content\"><div><span class=\"watupro_num\">4. <\/span>Which guideline makes more assumptions: ICH or ISO?<\/div><input type=\"hidden\" name=\"question_id[]\" id=\"qID_4\" value=\"135\" class=\"watupro-question-id\"><input type=\"hidden\" id=\"answerType135\" class=\"answerTypeCnt4\" value=\"radio\"><!-- end question-content--><\/div><div class=\"question-choices watupro-choices-columns \" id=\"questionChoices135\"><div class=\"watupro-question-choice  \" dir=\"auto\"><input type=\"radio\" name=\"answer-135[]\" id=\"answer-id-344\" class=\"answer   answerof-135 \" value=\"344\"><label for=\"answer-id-344\" id=\"answer-label-344\" class=\" answer\"><span><p>ICH<\/p><\/span><\/label><\/div><div class=\"watupro-question-choice  \" dir=\"auto\"><input type=\"radio\" name=\"answer-135[]\" id=\"answer-id-345\" class=\"answer   answerof-135 \" value=\"345\"><label for=\"answer-id-345\" id=\"answer-label-345\" class=\" answer\"><span><p>ISO<\/p><\/span><\/label><\/div><!-- end question-choices--><\/div><!-- end questionWrap--><\/div>\t\t\t\t\t<div style=\"display:none;\" id=\"liveResult-4\">\t\t   \n\t\t\t\t\t\t<img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\" alt=\"Loading...\" title=\"Loading...\">\u00a0Loading...\t\t\t\t\t<\/div>\t\n\t\t\t<\/div> \n\t   \t<p id=\"liveResBtn-135\" style=\"clear:both;\"><input type=\"button\" id=\"liveResultBtn135\" class=\"liveResultBtn4 watupro-live-result-btn\" value=\"See Answer\" onclick=\"WatuPRO.liveResult(135, 4);\"><\/p>\n\t   <div style=\"display:none\" id=\"question-5\">\n\t<div class=\"question-content\">\n\t\t<img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/img\/loading.gif\" width=\"16\" height=\"16\" alt=\"Loading...\" title=\"Loading...\">\u00a0Loading...\t<\/div>\n<\/div>\n\n<br>\n\t\n\t\t\t<div class=\"watupro_buttons flex \" id=\"watuPROButtons33\">\n\t\t  <div id=\"prev-question\" style=\"display:none;\"><input type=\"button\" value=\"&lt; Previous\" onclick=\"WatuPRO.nextQuestion(event, 'previous');\"><\/div>\t\t  \t\t  \t\t   \n\t\t   \t  \t\t<div><input type=\"button\" name=\"action\" class=\"watupro-submit-button\" onclick=\"WatuPRO.submitResult(event)\" id=\"action-button\" value=\"View Results\">\n\t\t<\/div>\n\t\t<\/div>\n\t\t\n\t<input type=\"hidden\" name=\"quiz_id\" value=\"33\" id=\"watuPROExamID\">\n\t<input type=\"hidden\" name=\"start_time\" id=\"startTime\" value=\"2026-04-19 05:32:44\">\n\t<input type=\"hidden\" name=\"start_timestamp\" id=\"startTimeStamp\" value=\"1776576764\">\n\t<input type=\"hidden\" name=\"question_ids\" value=\"\">\n\t<input type=\"hidden\" name=\"watupro_questions\" value=\"132: | 133: | 134:342,343 | 135:344,345\">\n\t<input type=\"hidden\" name=\"no_ajax\" value=\"0\">\t\t\t<\/form>\n\t<p>\u00a0<\/p>\n<\/div>\n\n<script type=\"text\/javascript\">\n\/\/jQuery(document).ready(function(){\ndocument.addEventListener(\"DOMContentLoaded\", function(event) { \t\nvar question_ids = \"132,133,134,135\";\nWatuPROSettings[33] = {};\nWatuPRO.qArr = question_ids.split(',');\nWatuPRO.exam_id = 33;\t    \nWatuPRO.post_id = 1183;\nWatuPRO.store_progress = 0;\nWatuPRO.curCatPage = 1;\nWatuPRO.requiredIDs=\"0\".split(\",\");\nWatuPRO.hAppID = \"0.55597600 1776565964\";\nvar url = \"https:\/\/sisu.ut.ee\/wp-content\/plugins\/watupro\/show_exam.php\";\nWatuPRO.examMode = 1;\nWatuPRO.siteURL=\"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-admin\/admin-ajax.php\";\nWatuPRO.emailIsNotRequired = 0;\nWatuPRO.perDecade = 10;\nWatuPROIntel.init(33);\nWatuPRO.inCategoryPages=1;});    \t \n<\/script>\n\n","protected":false},"excerpt":{"rendered":"","protected":false},"author":60,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_acf_changed":false,"inline_featured_image":false,"footnotes":""},"class_list":["post-1183","page","type-page","status-publish","hentry"],"acf":[],"_links":{"self":[{"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/pages\/1183","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/users\/60"}],"replies":[{"embeddable":true,"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/comments?post=1183"}],"version-history":[{"count":0,"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/pages\/1183\/revisions"}],"wp:attachment":[{"href":"https:\/\/sisu.ut.ee\/lcms_method_validation\/wp-json\/wp\/v2\/media?parent=1183"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}